2VX5
CELLVIBRIO JAPONICUS MANNANASE CJMAN26C MANNOSE-BOUND FORM
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-1 |
| Synchrotron site | ESRF |
| Beamline | ID23-1 |
| Temperature [K] | 100 |
| Collection date | 2006-12-03 |
| Spacegroup name | P 61 2 2 |
| Unit cell lengths | 84.712, 84.712, 244.687 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 41.740 - 1.470 |
| R-factor | 0.15136 |
| Rwork | 0.150 |
| R-free | 0.16871 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1j9y |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.144 |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.4.0076) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.520 |
| High resolution limit [Å] | 1.470 | 1.470 |
| Rmerge | 0.060 | 0.290 |
| Number of reflections | 804322 | |
| <I/σ(I)> | 47.4 | 5.3 |
| Completeness [%] | 99.1 | 91.7 |
| Redundancy | 9.1 | 7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
