2VT8
Structure of a conserved dimerisation domain within Fbox7 and PI31
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2004-01-06 |
Detector | MARRESEARCH |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 109.498, 45.212, 67.279 |
Unit cell angles | 90.00, 111.54, 90.00 |
Refinement procedure
Resolution | 28.090 - 2.600 |
R-factor | 0.206 |
Rwork | 0.203 |
R-free | 0.25600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PART-REFINED MODEL OF A L7M SEMET DERIVATIVE OBTAINED BY SAD PHASING |
RMSD bond length | 0.023 |
RMSD bond angle | 2.155 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.100 | 2.740 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.080 | 0.390 |
Number of reflections | 9607 | |
<I/σ(I)> | 20.1 | 4.1 |
Completeness [%] | 99.6 | 97.9 |
Redundancy | 7.1 | 6.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8 | 20% PEG 3350, 0.1 M AMMONIUM IODIDE, pH 8 |