2VSY

Xanthomonas campestris putative OGT (XCC0866), apostructure

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I03
Synchrotron site	Diamond
Beamline	I03
Temperature [K]	100
Detector technology	CCD
Collection date	2007-12-07
Detector	ADSC CCD
Spacegroup name	P 21 21 21
Unit cell lengths	81.523, 100.096, 156.274
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	20.000 - 2.100
R-factor	0.194
Rwork	0.193
R-free	0.23600
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.016
RMSD bond angle	1.597
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	AMoRE
Refinement software	REFMAC (5.4.0069)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	20.000	2.170
High resolution limit [Å]	2.100	2.100
Rmerge	0.090	0.470
Number of reflections	70020
<I/σ(I)>	14.8	4
Completeness [%]	93.5	86.1
Redundancy	4.3	4.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1