2VRP
Structure of rhodocytin
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE BM14 |
| Synchrotron site | ESRF |
| Beamline | BM14 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2007-12-08 |
| Detector | MARRESEARCH |
| Spacegroup name | I 2 2 2 |
| Unit cell lengths | 61.933, 89.368, 120.996 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 36.760 - 2.410 |
| R-factor | 0.204 |
| Rwork | 0.201 |
| R-free | 0.27200 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | COMPOSITE MODEL CONSISTING OF PDB ENTRY 1IOD PDB ENTRY 1J34 PDB ENTRY 1C3A PDB ENTRY 1UMR |
| RMSD bond length | 0.017 |
| RMSD bond angle | 1.916 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | BALBES |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.490 |
| High resolution limit [Å] | 2.400 | 2.400 |
| Rmerge | 0.040 | 0.120 |
| Number of reflections | 13367 | |
| <I/σ(I)> | 37.75 | 7.05 |
| Completeness [%] | 94.7 | 80.8 |
| Redundancy | 4 | 3.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 8 | 2M AMMONIUM SULPHATE, 5% 2-PROPANOL, pH 8 |
