2VQH
Crystal structure of PorB from Corynebacterium glutamicum (crystal form II)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS |
Synchrotron site | SLS |
Temperature [K] | 100 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 81.457, 81.457, 163.346 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 70.530 - 2.890 |
R-factor | 0.247 |
Rwork | 0.247 |
R-free | 0.25600 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 0.945 |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 70.530 | |
High resolution limit [Å] | 2.890 | |
Number of reflections | 7663 | |
<I/σ(I)> | 28.8 | 8.1 |
Completeness [%] | 99.2 | 100 |
Redundancy | 20.3 | 21.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |