2VQ1
anti trimeric Lewis X Fab54-5C10-A
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE BM14 |
| Synchrotron site | ESRF |
| Beamline | BM14 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2005-05-06 |
| Detector | MARRESEARCH |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 51.384, 161.015, 53.480 |
| Unit cell angles | 90.00, 103.07, 90.00 |
Refinement procedure
| Resolution | 25.000 - 2.500 |
| R-factor | 0.206 |
| Rwork | 0.203 |
| R-free | 0.26000 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1uz6 |
| RMSD bond length | 0.020 |
| RMSD bond angle | 1.668 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 28.700 | 2.640 |
| High resolution limit [Å] | 2.500 | 2.500 |
| Rmerge | 0.060 | 0.240 |
| Number of reflections | 29262 | |
| <I/σ(I)> | 18.5 | 5.2 |
| Completeness [%] | 99.9 | 100 |
| Redundancy | 3.7 | 3.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 4 | 0.1 M NA CITRATE PH 4, 11% PEG 3350 |
