2VP8

Structure of Mycobacterium tuberculosis Rv1207

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 5.0.3
Synchrotron site	ALS
Beamline	5.0.3
Temperature [K]	100
Detector technology	CCD
Collection date	2007-02-27
Detector	ADSC CCD
Spacegroup name	P 32 2 1
Unit cell lengths	80.727, 80.727, 215.938
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	19.840 - 2.640
R-factor	0.226
Rwork	0.223
R-free	0.26800
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1eye
RMSD bond length	0.008
RMSD bond angle	1.138
Data scaling software	SCALA
Phasing software	MOLREP
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	107.000	2.800
High resolution limit [Å]	2.640	2.640
Rmerge	0.070	0.450
Number of reflections	24807
<I/σ(I)>	8.5	1.6
Completeness [%]	99.3	99.2
Redundancy	3.2	3.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1