2VNF
MOLECULAR BASIS OF HISTONE H3K4ME3 RECOGNITION BY ING4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-09-12 |
Detector | ADSC CCD |
Spacegroup name | P 43 |
Unit cell lengths | 68.516, 68.516, 28.174 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 68.510 - 1.760 |
R-factor | 0.16 |
Rwork | 0.156 |
R-free | 0.22700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2g6q |
RMSD bond length | 0.012 |
RMSD bond angle | 1.816 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 68.510 | 1.810 |
High resolution limit [Å] | 1.760 | 1.760 |
Rmerge | 0.080 | 0.380 |
Number of reflections | 12178 | |
<I/σ(I)> | 9.9 | 1.7 |
Completeness [%] | 96.9 | 86.8 |
Redundancy | 3.8 | 2.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |