2VMH

The structure of CBM51 from Clostridium perfringens GH95

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Temperature [K]	113
Spacegroup name	P 65
Unit cell lengths	76.784, 76.784, 51.822
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	20.000 - 1.500
R-factor	0.15
Rwork	0.148
R-free	0.18400
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.019
RMSD bond angle	1.603
Phasing software	MOLREP
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	20.000	1.550
High resolution limit [Å]	1.500	1.500
Rmerge	0.060	0.400
Number of reflections	26520
<I/σ(I)>	13.4	3.4
Completeness [%]	99.8	99.9
Redundancy	6.5	5.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1