2VM3
Structure of Alcaligenes xylosoxidans in space group R3 - 1 of 2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SRS BEAMLINE PX10.1 |
Synchrotron site | SRS |
Beamline | PX10.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARRESEARCH |
Spacegroup name | H 3 |
Unit cell lengths | 89.941, 89.941, 143.732 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 68.520 - 1.800 |
R-factor | 0.186 |
Rwork | 0.184 |
R-free | 0.21000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1oe1 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.351 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 21.140 | |
High resolution limit [Å] | 1.800 | |
Rmerge | 0.060 | 0.240 |
Number of reflections | 36049 | |
<I/σ(I)> | 17.1 | 3.5 |
Completeness [%] | 94.5 | 79.6 |
Redundancy | 3.1 | 1.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | pH 6.5 |