2VL7

Structure of S. tokodaii Xpd4

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I03
Synchrotron site	Diamond
Beamline	I03
Temperature [K]	100
Detector technology	CCD
Collection date	2007-08-03
Detector	ADSC CCD
Spacegroup name	P 21 21 2
Unit cell lengths	95.713, 100.294, 62.488
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	29.700 - 2.250
R-factor	0.234
Rwork	0.232
R-free	0.27600
Structure solution method	MIRAS
Starting model (for MR)	NONE
RMSD bond length	0.010
RMSD bond angle	1.197
Data reduction software	DENZO
Data scaling software	SCALEPACK
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	29.700	2.330
High resolution limit [Å]	2.250	2.250
Rmerge	0.060	0.430
Number of reflections	27650
<I/σ(I)>	21.2	3
Completeness [%]	99.7	95
Redundancy	3.9	3.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1