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2VJI

Tailspike protein of E.coli bacteriophage HK620

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE ID14-2
Synchrotron siteESRF
BeamlineID14-2
Temperature [K]100
Detector technologyCCD
Collection date2001-10-08
DetectorADSC CCD
Spacegroup nameP 3 2 1
Unit cell lengths74.216, 74.216, 175.160
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution20.000 - 1.380
R-factor0.151
Rwork0.150
R-free0.18000
Structure solution methodSAD
Starting model (for MR)NONE
RMSD bond length0.009
RMSD bond angle1.499
Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwareSOLVE (RESOLVE V2.09)
Refinement softwareREFMAC (5.2.0005)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]20.0001.430
High resolution limit [Å]1.3801.380
Rmerge0.0600.260
Number of reflections115675
<I/σ(I)>12.75.1
Completeness [%]97.590.2
Redundancy4.64
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP3VAPOR DIFFUSION,HANGING DROP: PROTEIN CONCENTRATION 3MG/ML,5% PEG1500,PH3.0. RESERVOIR: 10% PEG 1500, PH 3.0. DROPLET 3 MICRO LITER: 3 MICRO LITER. CRYO CONDITION:30% PEG1500.

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