2VIU
INFLUENZA VIRUS HEMAGGLUTININ
Experimental procedure
Source type | SYNCHROTRON |
Source details | LURE BEAMLINE DW32 |
Synchrotron site | LURE |
Beamline | DW32 |
Detector technology | IMAGE PLATE |
Collection date | 1997-04-08 |
Detector | MARRESEARCH |
Spacegroup name | P 21 3 |
Unit cell lengths | 144.400, 144.400, 144.400 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 * - 2.500 |
R-factor | 0.213 * |
Rwork | 0.210 |
R-free | 0.23900 * |
RMSD bond length | 0.011 |
RMSD bond angle | 25.000 * |
Data reduction software | HKL |
Phasing software | X-PLOR (3.84) |
Refinement software | X-PLOR (3.84) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 2.450 |
Rmerge | 0.055 |
Total number of observations | 163053 * |
Number of reflections | 36234 |
Completeness [%] | 99.9 |
Redundancy | 4.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 70 (mg/ml) | |
2 | 1 | drop | 0.15 (M) | ||
3 | 1 | drop | 0.05 (%) | ||
4 | 1 | reservoir | citrate | 1.18 (M) | |
5 | 1 | reservoir | 0.05 (%) |