2VGD
Crystal structure of environmental isolated GH11 in complex with xylobiose and feruloyl-arabino-xylotriose
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 293 |
Detector technology | IMAGE PLATE |
Collection date | 2005-04-01 |
Detector | RIGAKU IMAGE PLATE |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 76.470, 76.470, 102.600 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.660 - 1.800 |
R-factor | 0.177 |
Rwork | 0.175 |
R-free | 0.20300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | APO FORM OF ENXYN11A |
RMSD bond length | 0.014 |
RMSD bond angle | 1.431 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 31.000 | 1.890 |
High resolution limit [Å] | 1.800 | 1.790 |
Rmerge | 0.090 | 0.750 |
Number of reflections | 27316 | |
<I/σ(I)> | 20.8 | 2 |
Completeness [%] | 99.8 | 99.6 |
Redundancy | 6.8 | 6.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.6 | 3.75 MM FAX3 0.2 M AMMONIUM FORMATE, PH 6.6 AND 17% (W/V) POLYETHYLENE GLYCOL 3350 |