2VG4

Rv2361 native

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID14-2
Synchrotron site	ESRF
Beamline	ID14-2
Temperature [K]	100
Detector technology	CCD
Detector	ADSC CCD
Wavelength(s)	0.933
Spacegroup name	P 32
Unit cell lengths	87.300, 87.300, 183.800
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	52.000 - 2.600
R-factor	0.23
Rwork	0.216
R-free	0.25500
Structure solution method	OTHER
Starting model (for MR)	NONE
Data reduction software	MOSFLM
Data scaling software	SCALA
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall
Low resolution limit [Å]	69.000
High resolution limit [Å]	2.600
Rmerge	0.140
Number of reflections	44230
<I/σ(I)>	8.4
Completeness [%]	84.0
Redundancy	2.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1