2VBY
Feast or famine regulatory protein (Rv3291c)from M. tuberculosis complexed with L-Tyrosine
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Temperature [K] | 298 |
| Detector technology | AREA DETECTOR |
| Detector | MARRESEARCH |
| Spacegroup name | P 42 21 2 |
| Unit cell lengths | 100.810, 100.810, 99.357 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 71.250 - 2.800 |
| R-factor | 0.205 |
| Rwork | 0.202 |
| R-free | 0.26100 |
| Structure solution method | MIRAS |
| Starting model (for MR) | NONE |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | SOLVE |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 2.950 |
| High resolution limit [Å] | 2.800 | 2.800 |
| Rmerge | 0.120 | 0.580 |
| Number of reflections | 12768 | |
| <I/σ(I)> | 11 | 2.8 |
| Completeness [%] | 97.9 | 99.9 |
| Redundancy | 4.9 | 4.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
