2VBS
Riboflavin kinase Mj0056 from Methanocaldococcus jannaschii in complex with PO4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARRESEARCH |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 77.700, 77.700, 107.070 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.990 - 3.000 |
R-factor | 0.232 |
Rwork | 0.230 |
R-free | 0.28200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2p3m |
RMSD bond length | 0.014 |
RMSD bond angle | 1.538 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.990 | 3.200 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.130 | 0.330 |
Number of reflections | 6951 | |
<I/σ(I)> | 8.43 | 4.39 |
Completeness [%] | 99.3 | 100 |
Redundancy | 4.28 | 4.43 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 2M NH4SO4 |