2VA0
Differential regulation of the xylan degrading apparatus of Cellvibrio japonicus by a novel two component system
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-4 |
| Synchrotron site | ESRF |
| Beamline | ID14-4 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2005-04-20 |
| Detector | ADSC CCD |
| Spacegroup name | P 21 21 2 |
| Unit cell lengths | 107.772, 80.014, 101.977 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 37.037 - 2.602 |
| R-factor | 0.202 |
| Rwork | 0.199 |
| R-free | 0.25880 |
| Structure solution method | SIRAS |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.019 |
| RMSD bond angle | 1.880 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | SHARP |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 37.560 | 2.740 |
| High resolution limit [Å] | 2.600 | 2.600 |
| Rmerge | 0.080 | 0.260 |
| Number of reflections | 27726 | |
| <I/σ(I)> | 3.06 | 1.34 |
| Completeness [%] | 99.9 | 100 |
| Redundancy | 5.69 | 4.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
