2V9T
Complex between the second LRR domain of Slit2 and The first Ig domain from Robo1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-01-26 |
Detector | ADSC CCD |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 51.270, 190.090, 40.870 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.980 - 1.700 |
R-factor | 0.188 |
Rwork | 0.186 |
R-free | 0.22600 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.015 |
RMSD bond angle | 1.565 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.800 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.080 | 0.530 |
Number of reflections | 42371 | |
<I/σ(I)> | 12.9 | 2.5 |
Completeness [%] | 98.1 | 94.9 |
Redundancy | 3.8 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.6 | 12% PEG 6000, 0.1M LI SO4, 0.1M NA CITRATE, PH=5.6 |