2V92
Crystal structure of the regulatory fragment of mammalian AMPK in complexes with ATP-AMP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 48.961, 121.032, 127.247 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.400 |
Rwork | 0.217 |
R-free | 0.25900 |
Structure solution method | MOLECULAR REPLACEMENT |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 2.400 |
Rmerge | 0.100 |
Number of reflections | 30415 |
<I/σ(I)> | 14.8 |
Completeness [%] | 99.7 |
Redundancy | 9.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |