2V8J

Structure of a Family 2 Pectate Lyase in Complex with a Transition Metal

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Temperature [K]	113
Spacegroup name	P 21 21 21
Unit cell lengths	68.180, 78.010, 104.200
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	20.010 - 2.010
R-factor	0.206
Rwork	0.203
R-free	0.24700
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.012
RMSD bond angle	1.250
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall
Low resolution limit [Å]	19.910
High resolution limit [Å]	2.000
Rmerge	0.090
Number of reflections	153616
Completeness [%]	93.2
Redundancy	4.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1