2V6Q
Crystal Structure of a BHRF-1 : Bim BH3 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
Synchrotron site | Australian Synchrotron |
Beamline | MX1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-06-22 |
Detector | ADSC QUANTUM 210r |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 62.736, 62.736, 92.523 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 35.220 - 2.700 |
R-factor | 0.208 |
Rwork | 0.206 |
R-free | 0.24900 |
Structure solution method | SIRAS |
Starting model (for MR) | NONE |
RMSD bond length | 0.015 |
RMSD bond angle | 1.663 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | HKL2Map |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.220 | 2.800 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.090 | 0.350 |
Number of reflections | 6089 | |
<I/σ(I)> | 27.8 | 3 |
Completeness [%] | 99.1 | 94.3 |
Redundancy | 7.2 | 5.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4 | 0.1 M MALIC ACID PH 4.0, 1.7 M NABR, 0.1 M GUANIDINE HCL |