2V3H
Thrombin with 3-cycle no F
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | ENRAF-NONIUS FR571 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 1999-11-30 |
| Detector | MARRESEARCH |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 70.440, 71.780, 72.410 |
| Unit cell angles | 90.00, 100.40, 90.00 |
Refinement procedure
| Resolution | 71.250 - 1.790 |
| R-factor | 0.175 |
| Rwork | 0.173 |
| R-free | 0.20700 |
| Structure solution method | OTHER |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.340 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | CCP4 |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.900 |
| High resolution limit [Å] | 1.790 | 1.790 |
| Rmerge | 0.040 | 0.210 |
| Number of reflections | 30755 | |
| <I/σ(I)> | 48.1 | 12.8 |
| Completeness [%] | 90.4 | 78 |
| Redundancy | 2.74 | 2.71 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
