Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL40B2 |
| Synchrotron site | SPring-8 |
| Beamline | BL40B2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2004-03-04 |
| Detector | ADSC CCD |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 33.629, 27.639, 70.967 |
| Unit cell angles | 90.00, 103.07, 90.00 |
Refinement procedure
| Resolution | 32.600 - 1.920 |
| R-factor | 0.184 |
| Rwork | 0.178 |
| R-free | 0.24000 |
| Structure solution method | MAD |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.423 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.980 |
| High resolution limit [Å] | 1.900 | 1.900 |
| Rmerge | 0.060 | 0.190 |
| Number of reflections | 9958 | |
| <I/σ(I)> | 24.2 | 8.4 |
| Completeness [%] | 98.9 | 93.2 |
| Redundancy | 3.1 | 2.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7 | PEG 6000, AMMONIUM CHLORIDE, PH 7.0 |
