Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL40B2 |
| Synchrotron site | SPring-8 |
| Beamline | BL40B2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2004-03-04 |
| Detector | ADSC CCD |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 151.781, 64.146, 68.018 |
| Unit cell angles | 90.00, 94.70, 90.00 |
Refinement procedure
| Resolution | 20.000 - 2.050 |
| R-factor | 0.254 |
| Rwork | 0.248 |
| R-free | 0.30800 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1om2 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.226 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 2.150 |
| High resolution limit [Å] | 2.050 | 2.050 |
| Rmerge | 0.050 | 0.400 |
| Number of reflections | 34455 | |
| <I/σ(I)> | 13.67 | 2.47 |
| Completeness [%] | 93.0 | 64.1 |
| Redundancy | 4.51 | 1.96 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 7 | PEG6000, AMMONIUM CHROLIDE, HEPES, PH 7.0, VAPOR DIFFUSION |
