2V12

Crystal Structure of Renin with Inhibitor 8

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	ENRAF-NONIUS FR571
Temperature [K]	10
Detector technology	AREA DETECTOR
Collection date	1993-01-01
Detector	DELFT
Spacegroup name	P 21 3
Unit cell lengths	142.900, 142.900, 142.900
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 - 3.200
R-factor	0.236
Rwork	0.236
Structure solution method	OTHER
RMSD bond length	0.018
RMSD bond angle	3.570
Data reduction software	MADNESS
Refinement software	X-PLOR

Data quality characteristics

	Overall
Low resolution limit [Å]	10.000
High resolution limit [Å]	3.200
Rmerge	0.130
Number of reflections	15411
Completeness [%]	92.0
Redundancy	2.81

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		4.5		pH 4.50