2UY7
Crystal structure of the P pilus rod subunit PapA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-02-25 |
Detector | ADSC CCD |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 166.960, 166.960, 178.010 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 75.800 - 2.600 |
R-factor | 0.2296 |
Rwork | 0.230 |
R-free | 0.26600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1pdk |
RMSD bond length | 0.007 |
RMSD bond angle | 1.354 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | AMoRE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 75.800 | 2.740 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.090 | 0.450 |
Number of reflections | 88336 | |
<I/σ(I)> | 7.3 | 1.7 |
Completeness [%] | 99.8 | 99.7 |
Redundancy | 5.2 | 5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.6 | 2M AMMONIUM SULFATE, 0.1M SODIUM ACETATE PH = 5.6 |