2UW8
Structure of PKA-PKB chimera complexed with 2-(4-chloro-phenyl)-2- phenyl-ethylamine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Temperature [K] | 100 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 72.318, 74.575, 80.011 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.620 - 2.000 |
R-factor | 0.188 |
Rwork | 0.185 |
R-free | 0.23300 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.025 |
Refinement software | REFMAC (5.2.0019G) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.600 | 2.110 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.070 | 0.320 |
Number of reflections | 27851 | |
<I/σ(I)> | 9.9 | 2.3 |
Completeness [%] | 98.5 | 98 |
Redundancy | 2.7 | 2.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |