2UUZ
Orthorhombic crystal form of GamS from bacteriophage lambda.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH3R |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 142.358, 39.147, 44.195 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 32.000 - 2.300 |
R-factor | 0.2403 |
Rwork | 0.240 |
R-free | 0.27920 |
Structure solution method | MIRAS |
RMSD bond length | 0.007 |
RMSD bond angle | 1.200 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SOLVE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.000 | 2.420 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.060 | 0.250 |
Number of reflections | 19530 | |
<I/σ(I)> | 7.3 | 3.1 |
Completeness [%] | 94.6 | 94.6 |
Redundancy | 4.7 | 5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.5 | 100 MM TRIS/HCL, PH 8.5 32-34 % PEG 4000 700-850 MM LICL |