2TGI

CRYSTAL STRUCTURE OF TRANSFORMING GROWTH FACTOR-BETA2: AN UNUSUAL FOLD FOR THE SUPERFAMILY

Experimental procedure

Spacegroup name	P 32 2 1
Unit cell lengths	60.600, 60.600, 75.300
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	15.000 * - 2.100 *
R-factor	0.172 *
RMSD bond length	0.016 *
RMSD bond angle	2.300 *
Refinement software	TNT

Data quality characteristics

	Overall
High resolution limit [Å]	2.100 *
Rmerge	0.047 *
Total number of observations	54248 *
Number of reflections	9706 *
Completeness [%]	87.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	acetate	10 (mM)
2	1	reservoir	PEG200	20 (%)
3	1	reservoir	sodium acetate	50 (mM)
4	1	reservoir	unbuffered sodium acetate	30-50 (mM)