2TDD
STRUCTURES OF THYMIDYLATE SYNTHASE WITH A C-TERMINAL DELETION: ROLE OF THE C-TERMINUS IN ALIGNMENT OF D/UMP AND CH2H4FOLATE
Experimental procedure
Spacegroup name | P 61 2 2 |
Unit cell lengths | 78.400, 78.400, 242.200 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | ? - 2.700 |
R-factor | 0.191 * |
Rwork | 0.190 |
RMSD bond length | 0.025 |
RMSD bond angle | 3.800 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 9999.000 * |
High resolution limit [Å] | 2.700 * |
Rmerge | 0.097 * |
Number of reflections | 10672 * |
Completeness [%] | 83.0 * |
Redundancy | 7.4 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | phosphate | ||
2 | 1 | drop | C-terminal valine | 5 (mg/mL) | |
3 | 1 | drop | ammonium sulfate | 1 (%sat) | |
4 | 1 | reservoir | phosphate | 1 (mL) | |
5 | 1 | reservoir | C-terminal valine | 5 (mg/mL) |