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2SGQ

GLN 18 VARIANT OF TURKEY OVOMUCOID INHIBITOR THIRD DOMAIN COMPLEXED WITH STREPTOMYCES GRISEUS PROTEINASE B AT PH 6.5

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU RU200
Temperature [K]287
Detector technologyAREA DETECTOR
DetectorSDMS
Spacegroup nameP 1 21 1
Unit cell lengths45.410, 54.700, 45.590
Unit cell angles90.00, 119.17, 90.00
Refinement procedure
Resolution20.000 - 1.800
Rwork0.149
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3sgb
RMSD bond length0.022
RMSD bond angle2.500
Refinement softwareTNT
Data quality characteristics
 Overall
Low resolution limit [Å]20.000
High resolution limit [Å]1.800
Rmerge0.089
Number of reflections17441
Completeness [%]89.0
Redundancy2.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
16.50.4 M SODIUM/POTASSIUM PHOSPHATE buffer AT PH 6.5

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PDB entries from 2024-11-20

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