2SGF
PHE 18 VARIANT OF TURKEY OVOMUCOID INHIBITOR THIRD DOMAIN COMPLEXED WITH STREPTOMYCES GRISEUS PROTEINASE B
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 287 |
Detector technology | AREA DETECTOR |
Detector | SDMS |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 45.580, 54.690, 45.670 |
Unit cell angles | 90.00, 119.17, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.750 |
Rwork | 0.137 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3sgb |
RMSD bond length | 0.022 |
RMSD bond angle | 3.500 |
Refinement software | TNT |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 1.750 |
Rmerge | 0.043 |
Number of reflections | 19032 |
Completeness [%] | 93.2 |
Redundancy | 2.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 0.4 M SODIUM/POTASSIUM PHOSPHATE AT PH 6.5 |