2SGD
ASP 18 VARIANT OF TURKEY OVOMUCOID INHIBITOR THIRD DOMAIN COMPLEXED WITH STREPTOMYCES GRISEUS PROTEINASE B AT PH 10.7
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 287 |
Detector technology | AREA DETECTOR |
Detector | SDMS |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 45.590, 54.610, 45.620 |
Unit cell angles | 90.00, 119.24, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.800 |
Rwork | 0.196 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3sgb |
RMSD bond length | 0.025 |
RMSD bond angle | 2.800 |
Refinement software | TNT |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 1.800 |
Rmerge | 0.105 |
Number of reflections | 17193 |
Completeness [%] | 88.0 |
Redundancy | 1.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 10.7 | 0.4M SODIUM/POTASSIUM PHOSPHATE BUFFER AT PH 10.7 |