2RTT

Solution structure of the chitin-binding domain of Chi18aC from Streptomyces coelicolor

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	DRX	Bruker DRX	500
2	Bruker	DRX	Bruker DRX	600
3	Bruker	DRX	Bruker DRX	800
4	Bruker	AVANCE	Bruker Avance	400

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-15N HSQC
10	1	1	2D 1H-15N HSQC
11	1	2	3D C(CO)NH
12	1	2	3D H(CCO)NH
13	1	1	3D 1H-15N NOESY
14	1	1	3D 1H-15N NOESY
15	1	5	2D DQF-COSY
16	1	5	2D 1H-1H NOESY
17	1	3	3D 1H-15N NOESY
18	1	2	3D 1H-13C NOESY
19	1	3	2D 1H-15N HSQC
2	1	2	2D 1H-15N HSQC
20	1	3	3D 1H-13C NOESY aromatic
21	1	2	4D H(CCO)NH
22	1	3	3D HCCH-TOCSY aromatic
3	1	2	3D HNCACB
4	1	2	3D CBCA(CO)NH
5	1	2	3D HNCO
6	1	2	3D HN(CA)CO
7	1	2	3D HBHA(CO)NH
8	1	1	3D 1H-15N TOCSY
9	1	2	2D 1H-13C HSQC

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	6	ambient	303

Conformers

Conformers Calculated Total Number	100
Conformers Submitted Total Number	30