Experimental procedure
Spacegroup name | C 2 2 21 |
Unit cell lengths | 76.800, 191.300, 63.400 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.300 |
R-factor | 0.2 |
RMSD bond length | 0.014 |
RMSD bond angle | 1.420 |
Phasing software | X-PLOR |
Refinement software | PROLSQ |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Microdialysis * | 7.5 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 4 (mg/ml) | |
2 | 1 | reservoir | 40 (%sat) | ||
3 | 1 | reservoir | Tris-borate-EDTA | 40 (mM) |