2RPT

Structure of the CC mismatch from the thymidylate synthase binding site 1 hairpin and analysis of its interaction with paromomycin

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	DRX	BRUKER DRX	600
2	Varian	INOVA	VARIAN INOVA	800

Experiment

experiment id	conditions id	solution id	Experiment type
1	2	1	2D 1H-1H NOESY
2	2	1	2D 1H-1H TOCSY
3	2	1	2D 1H-1H COSY
4	2	1	2D 1H-13C HSQC
5	2	2	3D 1H-13C NOESY-HSQC
6	2	2	3D HCCH-COSY
7	2	2	3D HCCH-TOCSY
8	1	2	2D 1H-15N HSQC
9	1	2	3D 1H-15N NOESY-HSQC

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1			278
2			293

Conformers

Conformers Calculated Total Number	50
Conformers Submitted Total Number	10