Experimental procedure
Spacegroup name | P 21 21 2 |
Unit cell lengths | 43.410, 85.992, 65.552 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.000 |
R-factor | 0.17 * |
Rwork | 0.170 |
RMSD bond length | 0.020 |
RMSD bond angle | 0.060 |
Refinement software | PROLSQ |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 2.000 |
Rmerge | 0.089 * |
Total number of observations | 51473 * |
Number of reflections | 13485 |
Completeness [%] | 90.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 5.8 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | ammonium sulfate | 47 (%) | |
2 | 1 | reservoir | phosphate | 0.1 (M) |