2RLP

NMR structure of CCP modules 1-2 of complement factor H

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	AVANCE	Bruker Avance	800
2	Bruker	AVANCE	Bruker Avance	600

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	2	2D 1H-15N HSQC
10	1	2	3D HCCH-TOCSY
11	1	2	3D H(CCO)NH
12	1	2	3D CBCANH
13	1	2	3D HBHANH
14	1	1	2D 1H-15N HSQC-IPAP-HN
15	1	2	2D 1H-15N HSQC-IPAP-HN
16	1	1	2D 1H-15N HSQC-IPAP-CAHA
17	1	2	2D 1H-15N HSQC-IPAP-CAHA
18	1	1	2D 1H-15N HNCO-IPAP-CACO
19	1	2	2D 1H-15N HNCO-IPAP-CACO
2	1	2	2D 1H-13C HSQC
20	1	3	2D 1H-15N HSQC
21	1	2	2D HBCBCGCDHD
22	1	2	2D HBCBCGCDCEHE
23	1	2	2D 1H-13C HSQC-CT aromatics
3	1	2	3D CBCA(CO)NH
4	1	2	3D C(CO)NH
5	1	2	3D HNCO
6	1	2	3D HNCACO
7	1	2	3D HBHA(CO)NH
8	1	2	3D 1H-13C NOESY
9	1	2	3D 1H-15N NOESY

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	6.2	ambient	310

Conformers

Conformers Calculated Total Number	100
Conformers Submitted Total Number	30