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2RL2

Crystal structure of UDP-N-acetylglucosamine enolpyruvyl transferase from Haemophilus influenzae in complex with UDP-N-acetylglucosamine and fosfomycin

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPHOTON FACTORY BEAMLINE BL-18B
Synchrotron sitePhoton Factory
BeamlineBL-18B
Temperature [K]100
Detector technologyCCD
Collection date2004-06-22
DetectorADSC QUANTUM 4
Wavelength(s)1.000
Spacegroup nameI 2 2 2
Unit cell lengths63.694, 124.463, 126.276
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution20.000 - 2.300
Rwork0.187
R-free0.23300
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareCNS
Refinement softwareCNS
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]20.0002.320
High resolution limit [Å]2.2002.200
Rmerge0.1000.231
Number of reflections25235
Completeness [%]97.999.7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP2961.8M ammonium sulfate, 5-10% glycerol, VAPOR DIFFUSION, HANGING DROP, temperature 296K

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