2RKM
STRUCTURE OF OPPA COMPLEXED WITH LYS-LYS
Experimental procedure
Source type | SYNCHROTRON |
Source details | SRS BEAMLINE PX9.5 |
Synchrotron site | SRS |
Beamline | PX9.5 |
Temperature [K] | 120 |
Detector technology | IMAGE PLATE |
Collection date | 1996-08-04 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 110.470, 77.150, 71.590 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.800 |
R-factor | 0.167 * |
Rwork | 0.167 |
R-free | 0.20200 * |
RMSD bond length | 0.006 |
RMSD bond angle | 0.022 |
Data reduction software | DENZO |
Data scaling software | SCALA |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.890 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.072 | 0.219 |
Total number of observations | 379533 * | |
Number of reflections | 57099 | |
<I/σ(I)> | 7.6 | 3.4 |
Completeness [%] | 92.9 | 98.9 * |
Redundancy | 6.6 | 5.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 5.5 | 7% PEG 4K, 50MM SODIUM ACETATE PH5.5, 1MM URANYL ACETATE AND 30MG/ML OPPA |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 25 (mg/ml) | |
2 | 1 | drop | sodium acetate | 50 (mM) | |
3 | 1 | reservoir | PEG4000 | 6 (%) | |
4 | 1 | reservoir | uranyl acetate | 1 (mM) |