2RKE
The Structure of rat cytosolic PEPCK in complex with sulfoacetate.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH3R |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2007-08-08 |
Detector | RIGAKU RAXIS IV++ |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 45.180, 119.031, 60.885 |
Unit cell angles | 90.00, 108.84, 90.00 |
Refinement procedure
Resolution | 29.090 - 1.800 |
R-factor | 0.205 |
Rwork | 0.203 |
R-free | 0.24900 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.237 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 100.000 | 100.000 | 1.860 |
High resolution limit [Å] | 1.800 | 3.880 | 1.800 |
Rmerge | 0.094 | 0.053 | 0.522 |
Number of reflections | 53184 | ||
<I/σ(I)> | 13.1 | ||
Completeness [%] | 94.7 | 99.7 | 70.2 |
Redundancy | 8.5 | 9.9 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.4 | 298 | 12-30% PEG 3350, 0.1M HEPES, 10 MM MNCL2, pH 7.4, temperature 298K, VAPOR DIFFUSION, HANGING DROP |