2RJY
Crystal structure of villin headpiece, P21 21 21 space group
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 95 |
Detector technology | IMAGE PLATE |
Collection date | 2004-06-10 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 31.212, 37.780, 53.147 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 13.460 - 1.400 |
R-factor | 0.209 |
Rwork | 0.209 |
R-free | 0.23300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | CRYSTAL STRUCTURE OF HP67 PDB ID: 1YU5 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.400 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 100.000 | 1.450 |
High resolution limit [Å] | 1.400 | 1.400 |
Number of reflections | 12685 | |
<I/σ(I)> | 34.3 | 5.6 |
Completeness [%] | 97.7 | 92.5 |
Redundancy | 6.1 | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 298 | PEG 8000, pH 6.50, VAPOR DIFFUSION, HANGING DROP, temperature 298K |