2RJB
Crystal structure of uncharacterized protein YdcJ (SF1787) from Shigella flexneri which includes domain DUF1338. Northeast Structural Genomics Consortium target SfR276
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X4C |
Synchrotron site | NSLS |
Beamline | X4C |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2007-08-10 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 0.97900 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 192.209, 76.387, 159.052 |
Unit cell angles | 90.00, 116.55, 90.00 |
Refinement procedure
Resolution | 41.120 - 2.600 |
R-factor | 0.233 |
Rwork | 0.233 |
R-free | 0.28100 |
Structure solution method | SAD |
RMSD bond length | 0.007 |
RMSD bond angle | 1.300 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SHELXD |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.690 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.072 | 0.228 |
Number of reflections | 64525 | |
<I/σ(I)> | 11.3 | 10 |
Completeness [%] | 98.9 | 98.5 |
Redundancy | 3.9 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | MICROBATCH UNDER OIL | 7 | 277 | NH4H2PO4, 0.1M MOPS, 20% PEG 1000, pH 7.0, MICROBATCH UNDER OIL, temperature 277K |