2RHF
D. radiodurans RecQ HRDC domain 3
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-10-26 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.9999, 0.9797 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 49.978, 49.978, 83.610 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.100 |
R-factor | 0.17798 |
Rwork | 0.177 |
R-free | 0.19399 |
Structure solution method | MAD |
RMSD bond length | 0.010 |
RMSD bond angle | 1.226 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | DM |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 83.600 | 1.160 |
High resolution limit [Å] | 1.100 | 1.100 |
Number of reflections | 40879 | |
<I/σ(I)> | 1.8 | |
Completeness [%] | 96.6 | 78.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4 | 273 | 1.8 M Na-K Phosphate pH 4.0, 0.1 M HEPES, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 273K |