2RF1
Crystal structure of ChoX in an unliganded closed conformation
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | EMBL/DESY, HAMBURG BEAMLINE BW7A |
| Synchrotron site | EMBL/DESY, HAMBURG |
| Beamline | BW7A |
| Detector technology | CCD |
| Collection date | 2007-04-04 |
| Detector | MAR CCD 165 mm |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 30.900, 196.200, 42.800 |
| Unit cell angles | 90.00, 90.10, 90.00 |
Refinement procedure
| Resolution | 10.000 - 2.000 |
| R-factor | 0.172 |
| R-free | 0.23500 |
| Structure solution method | AB INITIO |
| RMSD bond length | 0.001 |
| RMSD bond angle | 0.013 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | SHELX |
| Refinement software | SHELX |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 20.000 |
| High resolution limit [Å] | 1.600 |
| Rmerge | 0.104 |
| Number of reflections | 66140 |
| Redundancy | 3.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 5.1 | 277 | 0.1 Na acetate pH 5.1, 22% PEG 3350, VAPOR DIFFUSION, HANGING DROP, temperature 277K, pH 5.10 |
