2RDC
CRYSTAL STRUCTURE OF A PUTATIVE LIPID BINDING PROTEIN (GSU0061) FROM GEOBACTER SULFURREDUCENS PCA AT 1.80 A RESOLUTION
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.2 |
Synchrotron site | ALS |
Beamline | 8.2.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-08-31 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.0000, 0.9797, 0.9796 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 49.190, 116.250, 97.310 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.050 - 1.800 |
R-factor | 0.194 |
Rwork | 0.193 |
R-free | 0.22400 |
Structure solution method | MAD |
RMSD bond length | 0.017 |
RMSD bond angle | 1.405 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SHELX |
Refinement software | REFMAC (5.3.0040) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 29.050 | 29.050 | 1.860 |
High resolution limit [Å] | 1.800 | 3.870 | 1.800 |
Rmerge | 0.042 | 0.016 | 0.644 |
Number of reflections | 26165 | 4974 | 4460 |
<I/σ(I)> | 12.31 | 37 | 1.2 |
Completeness [%] | 99.0 | 98.6 | 95.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.07 | 277 | NANODROP, 28.6% 2-Methyl-2,4-pentanediol, 0.2M Lithium sulfate, 0.1M MES pH 6.07, VAPOR DIFFUSION, SITTING DROP, temperature 277K |