2RAC
AMICYANIN REDUCED, PH 7.7, 1.3 ANGSTROMS
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 273 |
Detector technology | AREA DETECTOR |
Detector | XUONG-HAMLIN MULTIWIRE |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 28.750, 56.200, 27.420 |
Unit cell angles | 90.00, 96.12, 90.00 |
Refinement procedure
Resolution | 6.000 - 1.300 |
R-factor | 0.182 |
Rwork | 0.182 |
R-free | 0.21000 |
Structure solution method | OTHER |
Starting model (for MR) | 1aac |
RMSD bond length | 0.007 |
RMSD bond angle | 27.500 * |
Data reduction software | UCSD-system |
Data scaling software | UCSD-system |
Phasing software | X-PLOR |
Refinement software | X-PLOR (3.843) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.040 | 1.450 |
High resolution limit [Å] | 1.300 | 1.300 |
Rmerge | 0.059 | 0.160 |
Number of reflections | 19838 | |
<I/σ(I)> | 13 | 2 |
Completeness [%] | 93.0 | 81 |
Redundancy | 5.2 | 3.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 4.38 * | macroseeding * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | phosphate | 3 (M) | |
2 | 1 | reservoir | sodium monobasic | 90 (%) | |
3 | 1 | reservoir | potassium dibasic | 10 (%) |