2R94
Crystal Structure of KD(P)GA from T.tenax
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-03-20 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.98 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 149.760, 149.760, 173.470 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.950 - 2.200 |
R-factor | 0.188 |
Rwork | 0.185 |
R-free | 0.22500 |
Starting model (for MR) | 1w3n |
RMSD bond length | 0.019 |
RMSD bond angle | 1.801 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.950 | 2.500 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.086 | 0.230 |
Number of reflections | 100096 | |
<I/σ(I)> | 14.48 | 5.02 |
Completeness [%] | 100.0 | 100 |
Redundancy | 9.8 | 10 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7 | 298 | HEPES/KOH, pH 7, vapor diffusion, temperature 298K |