2R8E
Crystal structure of YrbI from Escherichia coli in complex with Mg
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 21-ID-D |
| Synchrotron site | APS |
| Beamline | 21-ID-D |
| Detector technology | CCD |
| Collection date | 2007-02-02 |
| Detector | MARMOSAIC 225 mm CCD |
| Wavelength(s) | 0.97869 |
| Spacegroup name | P 1 |
| Unit cell lengths | 82.877, 83.005, 85.864 |
| Unit cell angles | 118.84, 118.77, 90.06 |
Refinement procedure
| Resolution | 29.340 - 1.400 |
| R-factor | 0.1601 |
| Rwork | 0.159 |
| R-free | 0.18807 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.368 |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 40.000 |
| High resolution limit [Å] | 1.400 |
| Number of reflections | 313166 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | 295 | pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 295K |
